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Naomi Bezdenejnih
Nashua, NH
(631) 988-9876
Naomi.Bezdenejnih@gmail.com
EDUCATION
The
Pennsylvania State University Eberly College of Science, University Park, PA
Bachelor
of Science in Chemistry, May 2007 (ACS-Certified Degree)
Lehigh
University, Bethlehem, PA
Masters
of Science in Chemistry, September 2012 (projected graduation date)
WORK
EXPERIENCE
AstraZeneca
RD Boston, Waltham, MA
Senior
Associate Scientist
(Analytical)
April
2009 – Present
- Screened,
optimized, and purified small-scale and large-scale chiral samples by HPLC
and SFC to support Infection IMED and Cancer IMED projects
- Performed
chiral purity determinations and QC analyses on enantiopure and purified
chiral samples
- Functioned
as the liaison for the RD Boston Chiral group to meet external chiral
separation needs of CROs and other AstraZeneca sites
- Developed
methods and purified large-scale achiral samples by SFC
- Executed
reversed-phase achiral purifications by HPLC
- Conducted
optical rotation analyses
- Repaired
and maintained analytical and preparative HPLC and SFC systems
- Aided
in the installations and qualifications of analytical and preparative SFC
systems
- Conceived
of and coordinated a sample transfer system with the Lab Services group
for the transportation of analytical samples within the RD Boston site
- Trained
and mentored co-workers on optical rotations, and chiral method
development and purification on HPLC and SFC systems
- Presented
research at professional conferences (see Publications section below for
details)
- Interviewed
prospective candidates for job opportunities within the Analytical group
- Represented
the Analytical group in a chemical safety committee
- Received
multiple awards for performance (See Awards section below for details)
Department
of Chemistry, Boston University, Boston, MA
Teaching
Fellow
September
2008 – December 2008
- Taught
basic organic laboratory techniques to undergraduate students for the
syntheses and purifications of small molecules
- Evaluated
students on introductory organic principles and laboratory practices
- Instructed
students on the use of instruments for the characterization of synthesized
products (GC, polarimeter, IR, melting point apparatus)
MPI
Research Inc. (formerly Exygen Research, Inc.), State College, PA
Research
Chemist Associate I
June
2007 – July 2008
- Conducted
GLP-based formulation, identification, and characterization studies on
commercial and non-commercial compounds via HPLC and LC/MS in a CRO
laboratory
- Perfected
multi-tasking skills that allowed for the undertaking of various projects
of differing disciplines simultaneously
- Analyzed
samples and processed data for the completion of studies independent of
SD/PI intervention
- Wrote
reports and certificates of analysis based on data obtained in studies
- Drafted
and revised methods of analysis for HPLC-guided studies
- Qualified
and troubleshot HPLCs for routine and non-routine maintenance
- Provided
training, mentoring, and tutelage to coworkers on the physical techniques
and theoretical concepts important to the common procedures of the
laboratory
- Interacted
daily with QA/QC unit for quick and thorough data evaluations and project
completions
Supelco,
Bellefonte, PA
Liquid
Separations Intern
January
2007 – May 2007
- Developed
packing methods for experimental HPLC stationary phases
- Synthesized
experimental stationary phases
- Carried
out application work and theoretical studies on experimental and
commercial HPLC columns
Department
of Chemistry, Pennsylvania State University, University Park, PA
Research
Assistant (Advisor: Dr. Blake Peterson)
September
2005 – January 2007
- Synthesized
novel small molecule androgen receptor antagonists for biological
evaluation
- Purified
lead analogues via standard techniques such as flash and preparative thin
layer chromatography
- Characterized
all products by LC-MS and FT-NMR methods
Forest
Laboratories, Inc., Hauppauge, NY
Medicinal
Chemistry Intern
May
2006 – August 2006
- Designed
and synthesized possible MCH-1 antagonists for the treatment of obesity
and metabolic disorders
- Isolated
analogues by preparative LC-MS and flash chromatography
Department
of Chemistry, Pennsylvania State University, University Park, PA
Chemistry
Tutor
September
2005 – May 2006
- Helped
undergraduate students understand important concepts in the general,
organic, and analytical chemistry courses
Forest
Laboratories, Inc., Hauppauge, NY
Chemical
Development/Medicinal Chemistry Intern
May
2005 – August 2005
- Developed
a key intermediate in a new synthetic route for an active ingredient in a
pharmaceutical
- Synthesized
several compounds to screen for potential CCR1 antagonists for
inflammatory disease treatment
- Analyzed
and purified commercial drugs and analogues via LC-MS and HPLC
SOFTWARE
KNOWLEDGE
- SFCPronto,
MassWare, ChemStation, MassLynx, FractionLynx, Empower, UniPoint,
Trilution
- 1D
NMR Processor, pKa dB (ACDLabs software)
- E-Notebook,
IBIS Data Capture, IBIS Explore
- MS
Office with extensive use in Excel, Word, and PowerPoint
- Beilstein/Gremlin,
SciFinder Scholar
- ChemDraw,
ISIS/Draw, ChemSketch
- Spartan
MM, Mathematica
TECHNICAL
SKILLS
- HPLC
- SFC
- LC-MS
- FT-NMR
Spectroscopy
- Thin-Layer
Chromatography
- FT-IR
Spectroscopy
- UV/Vis
Spectroscopy
- Gas
Chromatography
- Flash
Chromatography
- Fluorescence
Spectroscopy
- Polarimetry
- Multi-step
Synthesis
AWARDS
Award
Received: “On The Spot” award
Year:
2011
Reason
for Award: For the speed and quality of a large-scale chiral separation
performed for the Cancer IMED
Location:
AstraZeneca RD Boston
Award
Received: “On The Spot” award
Year:2011
Reason
for Award: For the speed and quality of a chiral separation for a particular compound
prior to toxicology studies; for determining that said sample was light
sensitive; for maintaining the busy chiral queue of Infection IMED projects,
while actively completing purification of said sample
Location:
AstraZeneca RD Boston
PUBLICATIONS
Medium:
Poster
Title:
Use of Amine Additive in the Sample Diluent in a Supercritical Fluid
Chromatography (SFC) Purification
Authors:
Natascha Bezdenejnih-Snyder, Valerie Hoesch, Nancy DeGrace
Location:
Chirality 2012, Hilton Fort Worth, Fort Worth, TX; PREP 2012, Hyatt Regency,
Cambridge, Boston, MA
Date:
To be presented in June 2012; July 2012
Medium:
Application Note
Title:
Use of Amine Additive in the Sample Diluent in a Supercritical Fluid
Chromatography (SFC) Purification
Authors:
Natascha Bezdenejnih-Snyder, Valerie Hoesch, Nancy DeGrace
Location:
LC/GC (The Application Notebook)
Date:
February 2012
Medium:
Poster
Title:
Using an Acetonitrile Mixture as a Polar Modifier in Normal-Phase Chiral HPLC
Purifications
Authors:
Natascha Bezdenejnih-Snyder, Valerie Hoesch, Milena Virrankoski, Nancy DeGrace
Location:
PREP 2011, Hyatt Regency Cambridge, Boston, MA
Date:
July 2011
Medium:
Poster
Title:
Factors That Can Lead to Successful Preparative SFC Separations
Author:
Natascha Bezdenejnih-Snyder
Location:
Conference Center at Waltham Woods, Waltham MA
Date:
June 2011 (Published and presented internally at AstraZeneca for
"Infection IMED Innovation Days")
TRAINING
COURSES
Course
Name: Preparative Chromatography for Intermediates and APIs
Hosts: Olivier Dapremont (AMPAC Fine Chemicals), Kathleen Mihlbachler (Bristol-Myers Squibb), Larry Miller (Amgen)
Location: Hyatt Regency Cambridge, Boston, MA
July 2011
Hosts: Olivier Dapremont (AMPAC Fine Chemicals), Kathleen Mihlbachler (Bristol-Myers Squibb), Larry Miller (Amgen)
Location: Hyatt Regency Cambridge, Boston, MA
July 2011
Course
Name: Supercritical Fluid Chromatography in the Pharmaceutical Industry
Hosts: Larry Miller (Amgen) and Larry Taylor (Virginia Tech University)
Location: Hynes Convention Center, Boston, MA
June 2010
Hosts: Larry Miller (Amgen) and Larry Taylor (Virginia Tech University)
Location: Hynes Convention Center, Boston, MA
June 2010
Course
Name: Using Small Particle Size and Unique Stationary Phases in UHPLC
Host: Darrel Zezzo (Restek)
Location: MPI Research, Inc., State College, PA
February 2008
Host: Darrel Zezzo (Restek)
Location: MPI Research, Inc., State College, PA
February 2008
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